反応 #1350587

反応方程式

methyl 2-methyl-3-nitrobenzoate

→

Methyl 3-Amino-2-methylbenzoate

溶媒

methanol

反応条件

後処理

1. 1
   ろ過the catalyst was filtered off
2. 2
   その他the solvent was removed

実験手順

210 g of methyl 2-methyl-3-nitrobenzoate (1.08 mol) were dissolved in 4 l of methanol, 21 g of Pd/C were added and the mixture was subsequently hydrogenated at ambient pressure. After the reaction had ended, the catalyst was filtered off and the solvent was removed. Yield: 178 g (quant.).

出典