反応 #1344314

反応方程式

2,5-diethoxycarbonyl-3,4-ethylenedioxythiophene

NaOH

→

2,5-dicarboxy-3,4-ethylenedioxythiophene

反応条件

後処理

1. 1
   温度The microwave reactor is heated by the 2.45 GHz microwave at a power of 500-1200 W
2. 2
   その他hydrolysis reaction for no more than 20 minutes

実験手順

The 2,5-diethoxycarbonyl-3,4-ethylenedioxythiophene and NaOH are mixed in the microwave reactor. The microwave reactor is heated by the 2.45 GHz microwave at a power of 500-1200 W to perform hydrolysis reaction for no more than 20 minutes to obtain 2,5-dicarboxy-3,4-ethylenedioxythiophene. The reaction is shown in the chemical formula (D).

出典