反応 #1342565

反応方程式

behenic acid

behenyl alcohol

→

behenyl behenate

反応条件

後処理

1. 1
   その他A four-necked round-bottom flask equipped with a stirrer
2. 2
   その他an esterification reaction
3. 3
   その他The reaction product was purified with methyl ether

実験手順

A four-necked round-bottom flask equipped with a stirrer, a thermocouple, and a nitrogen inlet tube was charged with 1 mole of behenic acid per 1 mole of behenyl alcohol. The ingredients in the flask were heated at 130° C. for 3 hours under a nitrogen atmosphere, to carry out an esterification reaction. The reaction product was purified with methyl ether, to give behenyl behenate. Here, the resulting compound had an acid value of 0.1 mgKOH/g, and a hydroxyl value of 1.2 mgKOH/g.

出典