反応 #1277971

ord-50741cdd210a4d198527218adf03e46c

反応方程式

CCCCOP(=O)(OCCCC)OCCCC
TBPA
CC(N)(CO)CO
AMPD
CC(N)(CO)CO.CCCCOP(=O)(OCCCC)OCCCC
TBPA AMPD

反応物

試薬

なし

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

Reaction of TBPA with AMPD gives an TBPA/AMPD adduct. AMPD is sold in commerce by Angus. 37.2 mmol of TBPA was combined with 37.2 mmol of AMPD in 164.5 g of pure ethanol. The mixture is refluxed for 2 hours. The solvent was removed using a rotary evaporator to produce a white solid.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US08679990B2uspto-grants-2014_03