反応 #1277970
ord-580b6dff96b84b95b49292334f0d0c27
反応方程式
TBPA
AEEA
→
TBPA AEEA
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
Reaction of TBPA with AEEA gives an TBPA/AEEA adduct. AEEA is sold in commerce by Dow Chemical. 43.6 mmol of TBPA was added to a round bottom flask with 51.00 grams of pure toluene. The mixture is heated to reflux after which 43.6 mmol of AEEA was added dropwise and the solution refluxed for one hour. The toluene is removed using a rotary evaporator to produce a yellow solid.