反応 #1267095

反応方程式

1-hydroxy-4-hydroxymethylpyrazole

N-methyl-N-phenylcarbamoyl chloride

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title compound

Methyl-phenyl-carbamic acid 4-hydroxymethyl-pyrazol-1-yl ester

反応条件

後処理

1. 1
   その他The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (62%, oil)

実験手順

The title compound was prepared from 1-hydroxy-4-hydroxymethylpyrazole and N-methyl-N-phenylcarbamoyl chloride applying the general procedure 8. The crude product was purified by flash chromatography (Quad flash 12, EtOAc-heptane) (62%, oil).

出典