反応 #1265366

ord-a7d9a462b0cf4b75b180d0c552ebfe50

反応方程式

OCCn1ccnc1
2-(1H-imidazol-1-yl)ethanol
O=C(Cl)c1ccc2ccccc2c1
2-naphthoyl chloride
O=C(OCCn1ccnc1)c1ccc2ccccc2c1
2-(1H-imidazol-1-yl)ethyl 2-naphthalenecarboxylate
収率 81.0%

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他The procedure of Synthesis Example 1

実験手順

The procedure of Synthesis Example 1 was repeated except that 2-(1H-imidazol-1-yl)ethanol was used instead of the triethanolamine, and 2-naphthoyl chloride was used instead of the benzoyl chloride, to give 2-(1H-imidazol-1-yl)ethyl 2-naphthalenecarboxylate in a yield of 81%.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07276324B2uspto-grants-2007_10