反応 #1265363

ord-3f51572fa0854f66918e0302d48701d8

反応方程式

OCCN1CCOCC1
2-morpholinoethanol
O=C(Cl)c1ccc2ccccc2c1
2-naphthoyl chloride
O=C(OCCN1CCOCC1)c1ccc2ccccc2c1
2-morpholinoethyl 2-naphthalenecarboxylate
収率 95.0%

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他The procedure of Synthesis Example 1

実験手順

The procedure of Synthesis Example 1 was repeated except that 2-morpholinoethanol was used instead of the triethanolamine, and 2-naphthoyl chloride was used instead of the benzoyl chloride, to give 2-morpholinoethyl 2-naphthalenecarboxylate in a yield of 95%.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07276324B2uspto-grants-2007_10