反応 #1254

反応方程式

4-methylbenzoic acid

thionyl chloride

→

4-Methylbenzoyl chloride

反応条件

後処理

1. 1
   workup.DISTILLATIONafter excess thionyl chloride was distilled off

実験手順

4-Methylbenzoyl chloride was prepared in a conventional manner from 4-methylbenzoic acid and thionyl chloride and after excess thionyl chloride was distilled off, was used as the crude product in the side chain chlorination.

出典