反応 #1253208
ord-fb11b0cd2b134735807b142cc50ef4bc
反応方程式
water
acetic acid
water
1-methylpyrrolidine
→
piperidine acetate
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1濃縮concentration
実験手順
A stock solution of 1 molar piperidine acetate was prepared by mixing one equivalent of glacial acetic acid in an appropriate volume of water and slowly adding one equivalent 1-methylpyrrolidine. The pH of the stock solution is 7. The stock solution was diluted in an appropriate volume of water or acetonitrile to working concentration.