反応 #1253207

ord-ff058bb489964229afdd7fe923c54cbb

試薬

なし

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    濃縮concentration

実験手順

A stock solution of 1 molar methylpiperidine acetate was prepared by mixing one equivalent of glacial acetic acid in an appropriate volume of water and slowly adding one equivalent of 1-methylpiperidine. The pH of the solution is 7. The stock solution was diluted with an appropriate volume of water or acetonitrile to working concentration.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US06613508B1uspto-grants-2003_09