反応 #1231

反応方程式

methyl 4-[7-(1-adamantyl)-6-hydroxy-2-naphthyl]benzoate

methoxyethoxymethyl chloride

→

expected compound

収率 55.0%

methyl 4-[7-(1-adamantyl)-6-methoxyethoxymethoxy-2-naphthyl]benzoate

収率 55.0%

反応条件

実験手順

Following the basic procedure of Example 12, by reacting 980 mg (2.4 mmol) of methyl 4-[7-(1-adamantyl)-6-hydroxy-2-naphthyl]benzoate with 330 μl (28.6 mmol) of methoxyethoxymethyl chloride, 650 mg (55%) of the expected compound were obtained in the form of an oil.

出典