反応 #1212

ord-1fba45c98c28483dbc24abfca08ff922

反応方程式

O=C1CCCCCCCCCCCCCCCO1
cyclohexadecanolide
NCCO
ethanolamine
COC(=O)CCCCCCCCCCCCCCCOC1CCCCO1
methyl 16-(2-tetrahydropyranyloxy)hexadecanate
OCCNCCO
diethanolamine
OCCNCCCCCCCCCCCCCCCCOC1CCCCO1
title compound
OCCNCCCCCCCCCCCCCCCCOC1CCCCO1
16-(2-hydroxyethylamino)-1-(2-tetrahydropyranyloxy)hexadecane

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他respectively, in Preparation Example 37

実験手順

A reaction was conducted in the same manner as in Preparation Example 37 except that ethanolamine and methyl 16-(2-tetrahydropyranyloxy)hexadecanate were used in place of diethanolamine and cyclohexadecanolide, respectively, in Preparation Example 37, thereby obtaining the title compound (IId-4).

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05723497uspto-grants-1998_03