反応 #1192972
ord-48642f58e3b84aca8818938e77021646
反応方程式
hexafluorophosphoric acid
diphenyliodonium chloride
fluoroboric acid
→
diphenyliodonium hexafluorophosphate
収率 74.0%
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
The procedure of Example 1 was repeated for preparing an aromatic halonium salt using diphenyliodonium chloride. In this preparation, fluoroboric acid was replaced by 25 ml (60%) hexafluorophosphoric acid. There was obtained a 74% yield of diphenyliodonium hexafluorophosphate having a m.p. of 139°-141° C.