反応 #1173031
ord-363fa08194634b6280b5403a107ec2ca
溶媒
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
52.5 g (0.2 mol) of methyl 3-iodobenzoate were heated to reflux for 18 hours with 81 g (0.2 mol) of Lawesson reagent in 330 ml of xylene. By working-up in an analogous manner to that described in Example 1(B) there were obtained 47 g (84.4%) of O-methyl 3-iodothiobenzoate as a yellow evil-smelling oil which was used without further purification.