反応 #1158472
ord-a91520211dae4f728b081af8cc19488e
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
236faE (CAS Reg. No. 20193-67-3) has been prepared by reaction of 2,2,2-trifluoroethanol with carbonyl fluoride to give the intermediate, CF3CH2OCOF, which was in turn reacted with sulfur tetrafluoride at 150-200° C. to give the product as disclosed by Eisemann in U.S. Pat. No. 3,394,878.