反応 #1155

ord-8d8d9084812145079c62beccf28cf5f0

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

In the same manner as in Reference Example 1, 5-methoxysalicylaldehyde was reacted with methyl bromoacetate to yield methyl 2-formyl-4-methoxyphenoxyacetate (yield 86%), which was then recrystallized from acetone-hexane to yield colorless prisms having a melting point of 74° to 75° C.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05723479uspto-grants-1998_03