反応 #1152212

反応方程式

methyl-m-iodobenzoate

chlorine

→

methyl-m-iodobenzoate dichloride

溶媒

chloroform

反応条件

後処理

1. 1
   その他The resulting yellow solution was evaporated

実験手順

A solution of 5.0 g methyl-m-iodobenzoate in 70 ml chloroform was cooled to 0°-10° and treated with gaseous chlorine for 1 hour. The resulting yellow solution was evaporated to afford 6.2 g methyl-m-iodobenzoate dichloride as yellow needles, mp=108°-110°. IR: 5.83, 7.80, 8.00, 8.90, 9.18, 10.52, 11.12, 12.39, and 13.48.

出典