反応 #1135813

反応方程式

1-ethoxy-2-methyl-3-nitrobenzene

→

3-ethoxy-2-methylaniline

溶媒

ethanol

反応条件

後処理

1. 1
   ろ過The mixtures were filtered
2. 2
   濃縮the filtrates were concentrated

実験手順

A mixture of 1-ethoxy-2-methyl-3-nitrobenzene described in Reference Preparation example 2539.9 g, palladium-carbon (palladium 5%) 4 g and ethanol 200 mL was stirred at room temperature under hydrogen atmosphere for eighteen hours. The mixtures were filtered and the filtrates were concentrated to give 3-ethoxy-2-methylaniline 33.0 g.

出典