反応 #1121770

反応方程式

3-tert-butyldimethylsilyloxybenzoic acid

thionyl chloride

→

3-tert-Butyldimethylsilyloxybenzoyl chloride

反応条件

後処理

1. 1
   温度was heated
2. 2
   温度at reflux for 1 hr 30 min
3. 3
   濃縮The reaction mixture was concentrated under reduced pressure
4. 4
   その他to yield 5.77 parts of an oil

実験手順

Into a 100 mL round bottom flask a mixture of 5 parts of 3-tert-butyldimethylsilyloxybenzoic acid and 25 mL of thionyl chloride was heated at reflux for 1 hr 30 min. The reaction mixture was concentrated under reduced pressure to yield 5.77 parts of an oil.

出典