反応 #1106669

ord-f5ff3aa120644be0be915121f0436399

反応方程式

CN(C)CCNc1cccc2c1C(=O)c1cccc(Cl)c1C2=O
Compound 17
CN(C)CCNc1cccc2c1C(=O)c1cccc(Cl)c1C2=O
1-Chloro-5-(2-(dimethylamino)ethylamino)anthracene-9,10-dione
COCCN
2-methoxyethylamin
COCCNc1cccc2c1C(=O)c1cccc(NCCN(C)C)c1C2=O
2-(dimethylamino) ethylamino-5-(2-methoxy ethylamino)anthracene-9,10-dione

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他This product was used in the next step without any purification

実験手順

This procedure was carried out as described previously in step (a) of Example 15, using Compound 17 (0.25 g, 0.76 mmol) and 2-methoxyethylamin (0.66 mL, 7.6 mmol). This product was used in the next step without any purification. The structure of Compound 23 is given below:

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US08715944B2uspto-grants-2014_05