反応 #1106649

ord-7100b316dfe849aabf5c42c6b16eff45

反応方程式

CCOc1ccccn1
2-ethoxypyridine
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+]
LiTFSI
→
CCOc1ccccn1.O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+]
2-ethoxypyridine LiTFSI
収率 157.6%

反応物

CCOc1ccccn1
2-ethoxypyridine
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+]
LiTFSI

試薬

なし

反応条件

温度
50°CELSIUS
詳細条件
See reaction.notes.procedure_details.

実験手順

10 g of purified 2-ethoxypyridine and 7.77 g of LiTFSI were put into a round bottom flask and slowly stirred for 50 minutes under a nitrogen circumstance of 50° C., thereby obtaining 17.5 g of 2-ethoxypyridine-LiTFSI eutectic mixture.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US08715866B2uspto-grants-2014_05