反応 #1106647

ord-c96c84f9deb24b0c8262da476c9f6170

反応方程式

c1c[nH]cn1
imidazole
O=S(=O)([N-]S(=O)(=O)C(F)(F)C(F)(F)F)C(F)(F)C(F)(F)F.[Li+]
LiBETI
→
O=S(=O)([N-]S(=O)(=O)C(F)(F)C(F)(F)F)C(F)(F)C(F)(F)F.[Li+].c1c[nH]cn1
imidazole LiBETI
収率 129.3%

反応物

c1c[nH]cn1
imidazole
O=S(=O)([N-]S(=O)(=O)C(F)(F)C(F)(F)F)C(F)(F)C(F)(F)F.[Li+]
LiBETI

試薬

なし

反応条件

温度
50°CELSIUS
詳細条件
See reaction.notes.procedure_details.

実験手順

5.3 g of purified imidazole and 10 g of LiBETI were put into a round bottom flask and slowly stirred for 50 minutes under a nitrogen circumstance of 50° C., thereby obtaining 15.2 g of imidazole-LiBETI eutectic mixture.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US08715866B2uspto-grants-2014_05