反応 #1106645

ord-5deaa066f335434bad96507e8dfca8df

反応方程式

c1cn[nH]c1
pyrazole
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+]
LiTFSI
→
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+].c1cn[nH]c1
pyrazole LiTFSI
収率 137.4%

反応物

c1cn[nH]c1
pyrazole
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+]
LiTFSI

試薬

なし

反応条件

温度
30°CELSIUS
詳細条件
See reaction.notes.procedure_details.

実験手順

2.13 g of purified pyrazole and 3 g of LiTFSI were put into a round bottom flask and slowly stirred for 5 hours under a nitrogen circumstance of 30° C., thereby obtaining 5.1 g of pyrazole-LiTFSI eutectic mixture.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US08715866B2uspto-grants-2014_05