反応 #1106644

ord-eaa34ca9562e4e5fb277211aaab5e690

反応方程式

c1nc[nH]n1
1,2,4-triazole
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+]
LiTFSI
→
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+].c1nc[nH]n1
targeted eutectic mixture
収率 137.0%
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+].c1nc[nH]n1
1,2,4-Triazole LiTFSI
収率 137.0%

反応物

c1nc[nH]n1
1,2,4-triazole
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+]
LiTFSI

試薬

なし

反応条件

温度
70°CELSIUS
詳細条件
See reaction.notes.procedure_details.

実験手順

3.6 g of purified 1,2,4-triazole and 5 g of LiTFSI were put into a round bottom flask and slowly stirred for 4 hours under a nitrogen circumstance of 70° C., thereby obtaining 8.5 g of targeted eutectic mixture.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US08715866B2uspto-grants-2014_05