反応 #1106643

ord-c7c21d9897bb41fca3c57edbb966395d

反応方程式

c1c[nH]cn1
imidazole
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+]
LiTFSI
→
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+].c1c[nH]cn1
imidazole LiTFSI
収率 137.4%

反応物

c1c[nH]cn1
imidazole
O=S(=O)([N-]S(=O)(=O)C(F)(F)F)C(F)(F)F.[Li+]
LiTFSI

試薬

なし

反応条件

温度
40°CELSIUS
詳細条件
See reaction.notes.procedure_details.

実験手順

14.2 g of purified imidazole and 20 g of LiTFSI were put into a round bottom flask and slowly stirred for 2 hours under a nitrogen circumstance of 40° C., thereby obtaining 34 g of imidazole-LiTFSI eutectic mixture.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US08715866B2uspto-grants-2014_05