反応 #1095849

反応方程式

Urocanic acid

urocanic acid

→

3-(1H-Imidazol-4-yl)propionic acid

溶媒

MeOH

反応条件

後処理

1. 1
   ろ過filtered
2. 2
   濃縮the filtrate was concentrated under a reduced pressure
3. 3
   その他to give the objective product

実験手順

Urocanic acid (3-(1H-imidazol-4-yl)-acrylic acid) (138 mg, 1 mmol) was placed in a round-bottom flask and dist MeOH was added thereto until urocanic acid was completely dissolved. To this solution, 10% Pd/C (30 mg) was added, replaced with H2 and stirred. After five hours, the loss of raw materials was confirmed, filtered, and the filtrate was concentrated under a reduced pressure to give the objective product.

出典