反応 #10932

ord-b23c8ba54c484e1bafaf208e0e2e4633

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

Allyl 3-tetrahydropyrrolyl-2-butenoate was prepared (4.7 g, 68%) in the same manner as described in the above Example 1 (1) from allyl acetoacetate (5.0 g, 35.17 mmol) and pyrrolidine (8.8 mL, 105.51 mmol), and the obtained product was identified with the following 1H NMR data.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07094908B2uspto-grants-2006_08