反応 #1078221

ord-ad5cb4844d3d43a6a8870749f117bee4

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

2-[4-(2-Diethylaminoethoxy)benzyl]-2-(4-methoxy-benzenesulfonyl)hexanoic acid ethyl ester was prepared according to the general method as outlined in example 12. Starting from 2-(4-methoxy-benzenesulfonyl)hexanoic acid ethyl ester (4 g, 12.7 mmol) and (2-(4-chloromethyl-phenoxy)ethyl]diethylamine (3.38 g, 14 mmol). Yield 8.21 g crude (100%); brown oil; MS: 520.4 (M+H)+.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US06462073B2uspto-grants-2002_10