反応 #1076343

反応方程式

N-vinylpyrrolidinone

phenyl azide

→

1-phenyl triazole

溶媒

ethanol

反応条件

後処理

1. 1
   その他In the method of preparation
2. 2
   workup.WAITto stand in the dark for several weeks
3. 3
   温度Refluxing the reaction mixture

実験手順

In the method of preparation, the reaction between the N-vinylpyrrolidinone and the phenyl azide is carried out at room temperature in ethanol as solvent, and allowed to stand in the dark for several weeks, depending on the reactivity of the phenyl azides. Refluxing the reaction mixture eliminates the 5-(2-oxo-1-pyrrolidino) group and yields the 1-phenyl triazole.

出典