反応 #1073160

ord-9294e126bd8b47b9b7be998f2dfcd389

反応方程式

CCCCCCCCCCCCN
dodecylamine
Cl.N[C@H]1C(O)O[C@H](CO)[C@@H](O)[C@@H]1O
glucosamine hydrochloride
→
CCCCCCCCCCCCNC1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1N.Cl
N-Dodecyl-N-(2-amino-2-deoxy-glucopyranosyl)-amine hydrochloride

反応物

CCCCCCCCCCCCN
dodecylamine
Cl.N[C@H]1C(O)O[C@H](CO)[C@@H](O)[C@@H]1O
glucosamine hydrochloride

試薬

なし

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    workup.ADDITIONwere added
  2. 2
    その他the product precipitated
  3. 3
    抽出The solid was extracted three times
  4. 4
    workup.STIRRINGby stirring with ether
  5. 5
    ろ過filtered off with suction
  6. 6
    その他dried under a high vacuum

実験手順

46 g of dodecylamine were melted at 60° and 31 g of glucosamine hydrochloride were added, with stirring. After cooling to room temperature, the product precipitated. The solid was extracted three times by stirring with ether and filtered off with suction and then dried under a high vacuum.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04710491uspto-grants-1987_12