反応 #1073158

ord-f10767dfc78d4c6c802fb1156d989e2b

反応方程式

Cl.N[C@H]1C(O)O[C@H](CO)[C@@H](O)[C@@H]1O
glucosamine hydrochloride
→
CCCNC1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1N.Cl
N-Propyl-(2-amino-2-deoxy-D-glucopyranosyl)-amine hydrochloride

反応物

Cl.N[C@H]1C(O)O[C@H](CO)[C@@H](O)[C@@H]1O
glucosamine hydrochloride

試薬

なし

溶媒

CCCN
n-propylamine

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    温度the suspension was warmed to 70°, until a clear solution
  2. 2
    その他was formed
  3. 3
    その他the product precipitated

実験手順

21.5 g of glucosamine hydrochloride were suspended in 17.7 g of n-propylamine and the suspension was warmed to 70°, until a clear solution was formed. On cooling to room temperature, the product precipitated.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04710491uspto-grants-1987_12