反応 #10702

反応方程式

2,6-diisopropylaniline

pyridine

2,4-Ditertbutylphenol

NaOH

phenolate

→

phenol

2-(2′,6′-Diisopropylphenylazo)-4,6-ditertbutylphenol

溶媒

toluene

water

反応条件

実験手順

This phenol was prepared, as described for above, from a theoretical yield of 7.4 mmol of diazotized 2,6-diisopropylaniline and a phenolate solution comprised of 2,4-Ditertbutylphenol (1.42 g), water (15 mL), NaOH (0.5 g), pyridine (3 mL), and toluene (6 mL) Yield=0.98 g (36%).

出典