反応 #1058658
ord-8c4b3263c4b04675b6eb1f480e12df65
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1温度with cooling
- 2workup.WAITwas left
- 3workup.WAITstoppered at room temperature overnight
実験手順
To 0.7 g (8.52 millimoles) of 1-methylimidazole was added slowly and with cooling, 1.5 g of (16.2 millimoles) chloromethylthioacetate. The solution solidified in 10 minutes and was left stoppered at room temperature overnight.