反応 #10136

ord-f6f26e92084842f196349d3229d1ff9b

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他The product of the reaction, which
  2. 2
    その他was used without further purification

実験手順

3-(3-Chloro-benzylamino)-phthalic acid dimethyl ester (1.61 g, 4.8 mmol) was treated in the same manner as described above for the synthesis of 3-(2-methoxy-ethylamino)-phthalic acid. The product of the reaction, which contained a mixture of diacid and monomethyl esters, was used without further purification.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07091353B2uspto-grants-2006_08