反応 #1005958

反応方程式

2-nitro-4-trifluoromethylbenzaldehyde

2-(ethylsulfanyl)aniline

→

(2-ethylsulfanylphenyl) (2-nitro-4-trifluoromethylbenzylidene)amine

収率 96.3%

溶媒

toluene

反応条件

後処理

1. 1
   温度was refluxed for 4 hours
2. 2
   濃縮concentrated under reduced pressure
3. 3
   洗浄The resulting residue was washed with t-butyl methyl ether

実験手順

A mixture of 500 mg of 2-nitro-4-trifluoromethylbenzaldehyde, 349 mg of 2-(ethylsulfanyl)aniline and 4 ml of toluene was refluxed for 4 hours and then concentrated under reduced pressure. The resulting residue was washed with t-butyl methyl ether to obtain 777 mg of (2-ethylsulfanylphenyl) (2-nitro-4-trifluoromethylbenzylidene)amine.

出典