Réaction #992686

ord-e08f5efc7a6e4caaaed595895ce16a64

Équation de réaction

Nc1n[nH]c(N)n1
3,5-Diamino-1,2,4-triazole
O=C(O)C(F)(F)F
Trifluoroacetic acid
Nc1nc(N)[nH+][nH]1.O=C([O-])C(F)(F)F
3,5-Diamino-1,2,4-Triazolium TFA

Solvants

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Traitement

  1. 1
    AutreThe water was removed in vacuo
  2. 2
    Températurewith heating to approximately 90° C. for 4 hours

Mode opératoire

3,5-Diamino-1,2,4-triazole (1.50 g, 15.14 mmol) was dissolved in 5 ml of distilled water. Trifluoroacetic acid (1.12 ml, 15.14 mmol) was added via syringe at room temperature and the reaction was stirred at room temperature for 1 hour. The water was removed in vacuo with heating to approximately 90° C. for 4 hours.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US08012277B2uspto-grants-2011_09