Réaction #992679

Équation de réaction

Hydrazine monohydrate

Trifluoroacetic acid

→

Hydrazinium TFA

Solvants

water

Conditions de réaction

Traitement

1. 1
   workup.STIRRINGthe reaction was stirred at room temperature overnight
2. 2
   AutreThe water was removed in vacuo
3. 3
   Températurewith heating to 80° C.
4. 4
   Autreyielding product as a colorless liquid

Mode opératoire

Hydrazine monohydrate (4.41 ml, 90.9 mmol) was added via syringe to a 250-ml round-bottom flask containing 50 ml of distilled water with stirring at room temperature. Trifluoroacetic acid (7.0 ml, 90.9 mmol) was added via syringe and the reaction was stirred at room temperature overnight. The water was removed in vacuo with heating to 80° C., yielding product as a colorless liquid.

Source