Réaction #955933

Équation de réaction

methyl 2,4-dimethylbenzoate

hydrazine

→

2,4-dimethylbenzohydrazide

Solvants

MeOH

Conditions de réaction

Traitement

1. 1
   Températurethe mixture was heated
2. 2
   Températureunder reflux for 40 hours
3. 3
   AutreThen the mixture was evaporated
4. 4
   Autredried under vacuum

Mode opératoire

To a solution of methyl 2,4-dimethylbenzoate (2 g, 12.2 mmol) in MeOH (10 mL) was added anhydrous hydrazine (1.95 mL, 61 mmol) and the mixture was heated under reflux for 40 hours. Then the mixture was evaporated and dried under vacuum to give 2,4-dimethylbenzohydrazide as a white solid (2 g, 100%; MS (M+H, 165).

Source