Réaction #955916

Équation de réaction

5-(2,5-dimethylfuran-3-yl)-2H-1,2,4-triazole-3(4H)-thione

2-(bromomethyl)pyridine hydrobromide

→

2-((5-(2,5-dimethylfuran-3-yl)-1H-1,2,4-triazol-3-ylthio)methyl)pyridine

Rendement 70.0%

Conditions de réaction

Mode opératoire

Prepared in a similar manner to example 1 using 5-(2,5-dimethylfuran-3-yl)-2H-1,2,4-triazole-3(4H)-thione (example 7a) and 2-(bromomethyl)pyridine hydrobromide. Yield 70%. 1H NMR (500 MHz, CDCl3): δ 2.27 (s, 3H), 2.59 (s, 3H), 4.32 (s,2H), 6.35 (s, 1H), 7.28-7.29 (d, 1H), 7.35-7.36 (d, 1H), 7.75 (t, 1H) 8.62 (s, 1H). MS(M+H, 287).

Source