Réaction #9346

Équation de réaction

Sodium propanoate

2,6-dipropylphenol

→

phenol

2,6-dipropyl-4-propionylphenol

Solvants

Triflic Acid

Conditions de réaction

Traitement

1. 1
   AutreThe resulting waxy solid was purified by chromatography on silica gel

Mode opératoire

Sodium propanoate (0.88 g, 1.5 eq) and 2,6-dipropylphenol (1.09 g, 1.0 eq) were combined in Triflic Acid (5.0 g) as in Example 13, step 1. The resulting waxy solid was purified by chromatography on silica gel using ethyl acetate:hexanes:acetic acid (10:90:1) to give the titled phenol.

Source