Réaction #91963

Équation de réaction

3-methyl-4-[(2-methylpropan-2-yl)oxycarbonyl]morpholine-3-carboxylic acid

trifluoroacetic acid

→

3-methylmorpholine-3-carboxylic acid

Solvants

DCM

Conditions de réaction

Traitement

1. 1
   Concentrationconcentrated under the vacuum
2. 2
   AutreThe residue was used directly in next step without further purification

Mode opératoire

To a solution of 3-methyl-4-[(2-methylpropan-2-yl)oxycarbonyl]morpholine-3-carboxylic acid (Accela ChemBio Co., Ltd., CAS: 1052680-53-1, 50 mg, 0.2.0 mmol) in DCM (1 ml) was added trifluoroacetic acid (1 mL) dropwise at room temperature. The resulting mixture was stirred at room temperature for one hour and then concentrated under the vacuum. The residue was used directly in next step without further purification,

Source