Réaction #8431

ord-ca781ecdb6a54777a07a8ce4c7128b30

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Mode opératoire

The title compound was prepared from 4-bromo-1-(benzenesulfonyl)-1H-indole and 4-ethylpiperazine according to Method 1 to afford 129 mg (48%) of a white solid: 1H NMR (CD3OD) δ 7.94–6.81 (m, 10 H), 3.69–3.62 (m, 4 H), 2.34–3.26 (partly hidden) (m, 4 H), 3.14–3.04 (m, 2 H), 1.40 (t, J=7 Hz, 3 H); MS (ESI) 370.1 (M+H)+; Purity (HPLC) >95%.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US07087750B2uspto-grants-2006_08