Réaction #833515

Équation de réaction

3-Bromo-4-hydroxybenzaldehyde

allyl bromide

potassium carbonate

→

3-bromo-4-(2-propenyloxy)benzaldehyde

Solvants

acetone

Conditions de réaction

Traitement

1. 1
   TempératureAfter cooling
2. 2
   Filtrationthe solid was filtered off
3. 3
   Lavagewashed with acetone
4. 4
   ConcentrationAfter complete concentration of the organic phase
5. 5
   Autrethere was obtained an oily residue that
6. 6
   Autrewas used directly in the second step without further purification

Mode opératoire

3-Bromo-4-hydroxybenzaldehyde (20.1 g, 0.100 mol) and allyl bromide (14.5 g, 0.120 mol) were heated under reflux together with potassium carbonate (20.7 g, 0.150 mol) in 150 ml acetone (abs.) for 8 hours. After cooling, the solid was filtered off and washed with acetone. After complete concentration of the organic phase, there was obtained an oily residue that was used directly in the second step without further purification.

Source