Réaction #833510

Équation de réaction

Vanillin

allyl bromide

potassium carbonate

→

3-methoxy-4-(2-propenyloxy)benzaldehyde

Solvants

acetone

Conditions de réaction

Traitement

1. 1
   TempératureAfter cooling
2. 2
   Filtrationthe solid was filtered off
3. 3
   Lavagewashed with acetone
4. 4
   AutreA yellow oil was obtained
5. 5
   Concentrationafter a thorough concentration of the organic phases

Mode opératoire

Vanillin (20.0 g, 0.130 mol) and allyl bromide (19.9 g, 0.160 mol) were heated under reflux together with potassium carbonate (27.3 g, 0.200 mol) in 150 ml acetone (abs.) for 8 hours. After cooling, the solid was filtered off and washed with acetone. A yellow oil was obtained after a thorough concentration of the organic phases.

Source