Réaction #818314

Équation de réaction

triethylenetetramine

hydrochloric acid

→

triethylenetetramine tetrahydrochloride

Rendement 90.0%

Conditions de réaction

Traitement

1. 1
   AutreAlso provided

Mode opératoire

Also provided are the formation of triethylenetetramine quaternary salts. In an additional embodiment, a tribenzaldehyde protected intermediate is reacted with at least more than about three equivalents of aqueous hydrochloric acid, for example, to form triethylenetetramine tetrahydrochloride, which is precipitated in greater than about 90% yield and greater than about 98% purity from isopropanol.

Source