Réaction #81634

Équation de réaction

2-bromobenzaldehyde

ethylene glycol

p-toluenesulfonic acid·H2O

toluene

→

2-(2-Bromophenyl)-1,3-dioxolane

Conditions de réaction

Traitement

1. 1
   AutreA 12 L 3-necked flask fitted with an overhead stirrer

Mode opératoire

A 12 L 3-necked flask fitted with an overhead stirrer was charged with 2-bromobenzaldehyde (800 g, 4.324 moles), ethylene glycol (402.6 g, 6.485 moles), p-toluenesulfonic acid·H2O (3.95 g, 0.021 moles) and toluene (3.785 kg, 41.074 moles).

Source