Réaction #76417

ord-1040e15fbbf246af81fada7285e58ba9

Équation de réaction

C=Cc1ccccc1
Styrene
C=C(C)C(=O)OCC1CO1
glycidyl methacrylate
C=Cc1ccccc1C=C
divinyl-benzene
C=C(C)C(=O)OCC1CO1.C=Cc1ccccc1C=C
GMA DVB
→
C=C(C)C(=O)OCC1CO1.C=Cc1ccccc1
Styrene glycidyl Methacrylate

Réactifs

—
2,2′-azobis (2-amidinopropane dihydrochloride)
C=Cc1ccccc1
Styrene
C=C(C)C(=O)OCC1CO1
glycidyl methacrylate
C=Cc1ccccc1C=C
divinyl-benzene
—
( g )
C=C(C)C(=O)OCC1CO1.C=Cc1ccccc1C=C
GMA DVB

Réactifs

Aucun

Solvants

O
water

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Mode opératoire

Styrene (St; Wako Pure Chemicals. It was used after distillation under reduced pressure of 21.5 mmHg at 46° C.), glycidyl methacrylate (GMA; Wako Pure Chemicals. It was used after distillation under reduced pressure of 2 mmHg at 33° C.), divinyl-benzene (DVB; Tokyo Kasei), 2,2′-azobis (2-amidinopropane dihydrochloride) (V-50; Wako Pure Chemicals) and water were used in the following compositional formula: St/GMA/DVB/V-50/H20=1.2/1.8+0.3/0.04/0.06/110 (g)

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US06703207B2uspto-grants-2004_03