Réaction #75651

Équation de réaction

3,5-dichloroaniline

ethylglyoxalate

4-methylstyrene

trifluoroacetic acid

→

Compound 19

5,7-dichloro-4-p-tolyl-1,2,3,4-tetrahydroquinoline-2-carboxylic Acid Ethyl Ester

Solvants

acetonitrile

Conditions de réaction

Mode opératoire

Compound 19 was prepared by the basic process from 5.0 mmol 3,5-dichloroaniline, 5.5 mmol ethylglyoxalate solution (50% toluene), 15.0 mmol 4-methylstyrene and 5.0 mmol trifluoroacetic acid in 30.0 ml acetonitrile.

Source