Réaction #729935

ord-7f3d5835462644fd83bede484eded0be

Équation de réaction

Cl.NNc1ccc(OCc2ccccc2)cc1
(4-benzyloxy-phenyl)-hydrazine hydrochloride salt
O=C1CCOc2ccccc21
Chroman-4-one
c1ccc(COc2ccc3[nH]c4c(c3c2)COc2ccccc2-4)cc1
title compound
c1ccc(COc2ccc3[nH]c4c(c3c2)COc2ccccc2-4)cc1
8-benzyloxy-6,11-dihydro-5-oxa-11-aza-benzo[a]fluorene

Conditions de réaction

Conditions détaillées
See reaction.notes.procedure_details.

Mode opératoire

Following the procedure described in Example 4, using (4-benzyloxy-phenyl)-hydrazine hydrochloride salt and Chroman-4-one (2.93 g, 16.84 mmol) as the starting material, the title compound was prepared as a brown solid.

Source

DOI: 10.6084/m9.figshare.5104873.v1Brevet: US07696239B2uspto-grants-2010_04